ICAR Rheometer

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ICAR Rheometer

Purpose

Icar_1 The ICAR Rheometer is a rugged, portable instrument for measuring fundamental flow (rheological) properties of fresh concrete. The instrument was developed at the International Center for Aggregate Research (ICAR) located at The University of Texas at Austin to fill the need for a method to characterize the true flow behavior of concrete mixtures. The traditional methods of measuring slump or slump flow are not capable of characterizing the fundamental rheological properties of concrete that exist during the processes of mixing, transporting, and placement. As a result, the true performance of innovative concrete mixtures cannot be measured with these traditional slump-based methods. The ICAR Rheometer provides, for the first time, a low-cost and simple to operate instrument that can be used for:

  • Research and development to characterize the influence of new materials on concrete rheology
  • Optimizing mixture proportions so that the resulting concrete flows readily but is resistant to segregation (especially important for self-consolidating concrete)
  • On-site quality control

Principle

Fresh concrete can be considered as a fluid, which means that it will flow under the action of shear stresses. The flow behavior of concrete can be represented by the following two-parameter relationship:
Icar_2which is known as the Bingham model: The parameter τo is the yield stress, and it represents the shear stress required to initiate flow. The slope of the line is the plastic viscosity, µ, and it affects the resistance to flow after the yield stress has been surpassed. These two parameters, which define the flow curve, provide a complete description of the flow behavior of a fluid.
Icar_3Concrete, however, is not a simple fluid because it displays thixotropic behavior, which means that the shear stress required to initiate flow is high if the concrete has been in an “at rest” condition, but a lower shear stress is needed to maintain flow once it has begun. This type of behavior is summarized in the schematic plot shown above, which shows the variation in shear stress with time for the case of a low applied shear strain rate. At the start, the shear stress increases gradually with time but there is no flow. When the stress reaches the static yield stress, the concrete begins to flow and the stress required to maintain flow is reduced to the dynamic yield stress. If the applied shear strain rate is reduced to zero and the concrete is allowed to rest, inter-particle forces create a weak framework that restores the static yield stress. With time, the static and dynamic yield stresses increase as the effectiveness of water-reducing admixtures diminish and hydration proceeds, which is commonly referred to as “slump loss.”
Icar_4 The ICAR Rheometer is designed to characterize the static yield stress, the dynamic yield stress and plastic viscosity of the concrete. A high static yield stress is desirable because it reduces formwork pressure and increases the resistance to segregation. But for ease of pumping, placement, and self-consolidation, a low dynamic yield stress is necessary. The dynamic viscosity provides cohesiveness and contributes to reducing segregation when concrete is flowing. The schematic plot to the right shows dynamic flow curves for conventional concrete and different types of self-consolidating concrete (SCC) mixtures. The conventional concrete has a high dynamic yield stress and additional energy (vibration) is needed to consolidate the concrete after it is placed in forms. The self-consolidating mixtures all have low dynamic yield stress and will consolidate due to self-weight, but they have different rheological properties. The SCC with a high plastic viscosity (red line) will be sticky and difficult to place and strike off. On the other hand, the mixture with low plastic viscosity (green line) will be prone to segregation. Thus by determining the dynamic flow curves of concretes with different mixture proportions and type of admixtures, and optimum balance between ease of flow and resistance to segregation can be realized. These types of determinations cannot be done using conventional slump-based tests.

ICAR Plus Rheometer

The ICAR Plus Rheometer is the successor to the ICAR Rheometer. This device is provided with a stronger motor, digital based electronics and more comprehensive software. The main advantage of the ICAR Plus is its digital verification process, allowing users to always have a ready to use system under any environment and working condition. ICAR Plus will always be calibrated by the user on-site and can be verified in the laboratory with the same silicone as its predecessor ICAR Rheometer.
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Method of Operation

Icar_6 The ICAR Plus Rheometer is composed of a container to hold the fresh concrete, a driver head that includes an electric motor and torque meter; a four-blade vane that is held by the chuck on the driver; a frame to attach the driver/vane assembly to the top of the container; and a laptop computer to operate the driver, record the torque during the test, and calculate the flow curve parameters. The container contains a series of vertical rods around the perimeter to prevent slipping of the concrete along the container wall during the test. The size of the container and length of the vane shaft are selected based on the nominal maximum size of the aggregate. The vane diameter and height are both 127 mm.

Two types of tests are performed. The first type is a stress growth test in which the vane is rotated at a constant slow speed of 0.025 rev/s. The initial increase of torque is measured as a function of time. The maximum torque measured during this test is used to calculate the static yield stress. The other type of test is a flow curve test to determine the dynamic yield stress and the plastic viscosity. The flow curve test begins with a “breakdown” period in which the vane is rotated at maximum speed. This is done to breakdown any thixotropic structure that may exist and to provide a consistent shearing history before measuring the Bingham parameters. The vane speed is then decreased in a specified number of steps, which is selected by the user but at least six steps are recommended. During each step, the vane speed is held constant and the average speed and torque are recorded. The plot of torque versus speed of vane rotation defines the flow curve from which the Bingham parameters are calculated.

The ICAR Plus Rheometer software performs all the necessary functions: operates the driver, records the torque, computes test results, and stores data. The entire testing is controlled from a single screen as shown below. The user defines the test geometry and provides the test parameters to run the flow curve test. A simple press of the “Start” button initiates the stress growth test and flow curve test is started by pressing the second “Start” button. Both tests are completed within 1 minute.
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Example Results

The figure below on the left shows the results of a stress growth test. The program uses the peak torque and test geometry to calculate the static yield stress, which is displayed at the bottom of the computer display. The figure on the right shows the average torque versus average vane rotation measured during six steps of the flow curve test. The software computes a best-fit line to the data and reports the intercept and slope as relative parameters. Based on the test geometry, the software computes the Bingham parameters: dynamic yield stress and plastic viscosity.
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ICAR Plus Rheometer Specifications

  • Minimum slump: The concrete has to have a slump greater than 75 mm, otherwise the concrete is too stiff for testing by the apparatus
  • Nominal maximum size of aggregate: 32 mm for largest available container
  • Vane rotation speed: 0.001 to 0.667 rev/s
  • Motor type: Integrated Servo Motor
  • Minimum Torque: 0.01Nm
  • Peak Torque: 90Nm for not more than 2 seconds
  • Continuous Maximum Torque: 32Nm
  • Power Supply: Input of 100-240 VAC – 3.5A
  • Output of 48V – 6.7A. IP67
  • Digital Calibration can be performed by user anytime
  • Performs static stress growth test and dynamic flow curve tests
  • Software controls tests and computes static yield stress, dynamic yield stress, and plastic viscosity in fundamental units
  • Test time: 1 minute
  • Computer requirements: Windows 7 or higher. Processor I3 or higher
  • Motor drive dimensions: 11 x 11 x 43 cm
  • Motor console weigh: 7.5 kg
  • Carrying Case dimensions: 67 x 52 x 28 cm
  • Carrying Case weight: 20 kg, Including Motor Drive, Base Frame, Vane, Power Supply and Cables

RHM-4000 ICAR Plus Rheometer Kit Ordering Numbers

Packing

Item Order #
Motor drive/torque meter unit RHM-4001
Power cord for motor drive/torque meter unit RHM-4002
Base plate for attaching motor drive/torque meter unit to container RHM-3003
Container for 19 mm NMSA aggregate – standard (see below for other sizes) RHM-3005
Four-blade vane for 19 mm NMSA aggregate
Vane is 127 mm in height and diameter
Overall length depends on NMSA (see below for other sizes)
RHM-3009
USB cable to connect motor drive/torque meter unit to computer RHM-3012
Laptop computer with installed software RHM-4013
Software on CD-ROM RHM-4014
User manual RHM-4015
Carrying case for laptop computer RHM-4016
Carrying case for Rheometer and accessories
Container does not ship with case
Weight of case and Rheometer kit – 20 kg
RHM-4017
Silicone oil for verification of instrument (19 L) RHM-4018

Ordering numbers for container and vane for different nominal maximum size of aggregate (NMSA)

Nominal Maximum Size of Aggregate
12.5 mm 19.0 mm 25.0 mm 32 mm
Container
Diameter/Height
RHM-3004
280 mm/280 mm
RHM-3005*
305 mm/312 mm
RHM-3006
355 mm/380 mm
RHM-3007
405 mm/460 mm
Vane
Overall Length
RHM-3008
235 mm
RHM-3009*
240 mm
RHM-3010
290 mm
RHM-3011
330 mm

*Size provided if another size is not specified.

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